Atom probe analysis results of Co-22at%CR bulk alloy and its thin film
s are presented. While no compositional inhomogeneity is detected from
the bulk sample, a significant compositional fluctuation is present i
n the thin film specimen which is sputter deposited on a heated substr
ate. The concentration of the Cr enriched region is in the range of 30
- 40 at.%Cr, while that of the Cr depleted region is approximately 5
at.%Cr. Such compositional fluctuations are present within a grain. Th
ese results are in agreement with NMR and TEM results.