ANALYSIS OF METHYL NEODECANAMIDE IN LAKE WATER BY REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY AND GAS-CHROMATOGRAPHY MASS-SPECTROMETRY

Authors
RASMUSSEN HT FRIEDMAN SK MUSTILLI AJ MCDONOUGH R MCPHERSON BP
Citation
Ht. Rasmussen et al., ANALYSIS OF METHYL NEODECANAMIDE IN LAKE WATER BY REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY AND GAS-CHROMATOGRAPHY MASS-SPECTROMETRY, Journal of liquid chromatography, 17(3), 1994, pp. 589-601
Citations number
8
Categorie Soggetti
Chemistry Analytical
Journal title
Journal of liquid chromatography → ACNP
ISSN journal
01483919
Volume
17
Issue
3
Year of publication
1994
Pages
589 - 601
Database
ISI
SICI code
0148-3919(1994)17:3<589:AOMNIL>2.0.ZU;2-K
Abstract
Methyl Neodecanamide (MNDA) has been quantitated in lake water at leve ls of 0.1 to 1000 ppm. Total recoveries from spiked placebos were 99.8 +/- 2.3% at the 1000 ppm level and 98.3 +/- 4.3% at the 0.1 ppm level (based on 54 determinations at each level). Plots of actual concentra tions vs. determined concentrations were linear from 0.07 - 0.13 and 7 00 - 1300 ppm (r > 0.999). Stability of MNDA in lake water was verifie d by determining the composition by GC/MS immediately after dissolutio n and after 3 days.