In order to specify the relationship between the glass transition and
the deposits observed during spray-drying of carbohydrate solutions, m
easurements of glass transition temperatures (T-g) are made on pure su
gars or mixtures of sugars and starch hydrolysis products with a diffe
rential scanning calorimetry technique, whereas the stickiness is eval
uated through spray-drying trials performed in a pilot tower. The resu
lts show the influence of dextrose-equivalent and of molecular mass on
T-g, and the significant role of T-g on the deposits occuring during
spray-drying.