J. Tullis et Hr. Wenk, EFFECT OF MUSCOVITE ON THE STRENGTH AND LATTICE PREFERRED ORIENTATIONS OF EXPERIMENTALLY DEFORMED QUARTZ AGGREGATES, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 175(1-2), 1994, pp. 209-220
Axial compression experiments were performed on synthetic aggregates o
f quartz with varying volume percentages of muscovite, in order to ass
ess the effect of the muscovite on the flow strength and the lattice p
referred orientations. The experiments were performed at 800-degrees-C
, with a confining pressure of 1200 MPa, constant strain rates of 10(-
5) and 10(-6) s-1, and variable strains. At 10(-5) s-1, the quartz is
very strong and deforms by recrystallization-accommodated dislocation
creep. Experiments were carried out with 0%, 15%, 25%, 50% and 100% mu
scovite, using quartz grains 125-250 mum in size and muscovite grains
of less than 20 mum in size. The peak strength of the aggregates is ma
rkedly decreased by the addition of muscovite; it decays from 1400 MPa
(100% quartz) to 700 MPa (85%) to 450 MPa (50%) and then to 400 MPa (
100% muscovite). The decreasing composite strength correlates with a s
ignificant decrease in the quartz grain strain, because strain is part
itioned into the weaker muscovite, which undergoes kinking and dynamic
recrystallization in addition to basal slip. At 10(-6) s-1, the quart
z is much weaker and deforms by climb-accommodated dislocation creep.
Experiments were carried out with 0%, 25% and 50% muscovite, using qua
rtz grains 90-120 mum in size and muscovite grains 53-90 mu in size. U
nder these conditions, the addition of muscovite has a smaller effect
on the aggregate strength: it decays from 300 MPa (100% quartz) to 250
MPa (75%) to 200 MPa (50%). However, the quartz grain strain is signi
ficantly reduced by the muscovite additions. The quartz preferred orie
ntations were measured by time-of-flight neutron diffraction at LANSCE
for pure quartz samples and for those with 25% and 50% muscovite, sho
rtened 35% and 50%. The pure quartz aggregate developed a small circle
girdle of c axes. Adding 25% and 50% muscovite did not change the gen
eral texture pattern of the quartz but greatly reduced its strength, r
eflecting the reduced quartz grain strain and the greater strain heter
ogeneity.