Lm. Hsiung et Ns. Stoloff, LOW-ENERGY DISLOCATION-STRUCTURES IN CYCLICALLY DEFORMED NI3AL SINGLE-CRYSTALS, Acta metallurgica et materialia, 42(4), 1994, pp. 1457-1467
Low-energy dislocation structures in Ni3Al single crystals (oriented f
or single slip) fatigued at room temperature were studied using transm
ission electron microscopy. In general, dislocation structures in fati
gued Ni3Al were composed of primary superdislocations, edge superdislo
cation bundles (mutually trapped edge superdislocations), primary edge
superdislocation dipoles (line vector parallel-to [121BAR]), and faul
ted superdislocation dipoles (line vector parallel-to [110BAR] or para
llel-to [011BAR]). No wall or cell structure was observed. Paired prim
ary superdislocations, as they glided in the (111) slip plane during c
yclic deformation, were energetically unstable because of the fluctuat
ion of the separation between two superpartial dislocations (b = +/- 1
/2[101BAR]). The fluctuation led to an increase in the line energy of
the primary superdislocations, and resulted in the onset of several di
slocation reactions. Since the resulting dislocations of these reactio
ns were all sessile, their line energy remained unchanged during cycli
c deformation. Accordingly, they were considered to be energetically m
ore stable than primary superdislocations.