We demonstrate the use of Raman microscopy for leak detection in herme
tically sealed micromachined accelerometers. Leaks were indicated by t
he presence of a foreign gas, in this case oxygen, in the 70-mu m-deep
cavity enclosing the accelerometer between a silicon cap and a Pyrex(
R) window. Confocal, nondiffraction-limited operation of the Raman mic
roscope utilized the available pathlength in the sample while still re
jecting most of the fluorescence from the Pyrex(R), Raman peak intensi
ties were accurately determined in the presence of noise by fitting th
e spectra to a function that modeled the unresolved Q-branch line shap
es of oxygen and nitrogen.