IDENTIFICATION OF MODIFIED NATURAL PORPHYRIN ISOMERS - H-1 AND C-13 NMR ASSIGNMENTS BY NOESY AND REVERSE HETERONUCLEAR SHIFT CORRELATION

Citation
A. Bondon et al., IDENTIFICATION OF MODIFIED NATURAL PORPHYRIN ISOMERS - H-1 AND C-13 NMR ASSIGNMENTS BY NOESY AND REVERSE HETERONUCLEAR SHIFT CORRELATION, Magnetic resonance in chemistry, 32(2), 1994, pp. 78-82
Citations number
25
Categorie Soggetti
Spectroscopy,Chemistry
ISSN journal
07491581
Volume
32
Issue
2
Year of publication
1994
Pages
78 - 82
Database
ISI
SICI code
0749-1581(1994)32:2<78:IOMNPI>2.0.ZU;2-V
Abstract
The efficiency of two-dimensional homonuclear H-1-H-1 NOE spectroscopy in characterizing and fully assigning the H-1 NMR spectra of several isomers of meso- or ring-substituted deuteroporphyrins is demonstrated . The carbon resonances of the skeleton and the substituents were full y assigned using two-dimensional reverse heteronuclear shift correlati on spectroscopy.