C. Kim et al., LOW-DIMENSION STRUCTURAL-PROPERTIES AND MICROINDENTATION STUDIES OF ION-BEAM-SPUTTERED MULTILAYERS OF AG AL FILMS/, Thin solid films, 240(1-2), 1994, pp. 52-55
Artificially modulated silver/aluminum multilayer films with modulatio
n wavelengths LAMBDA between 1.35 and 21.3 nm, and total film thicknes
ses of 1 mum were prepared by ion-beam sputtering. The mechanical prop
erties of these films were investigated by a low load microhardness in
dentation technique. The films displayed increased hardness as the mod
ulation wavelength decreased. X-ray diffraction scans showed well-defi
ned small angle peaks and satellite peaks for high angles indicating a
coherent multilayer structure. The hardness enhancement as the modula
tion wavelength decreases may be partially attributed to the Ag2Al for
mation at the interfaces. The high quality of the well-defined layer s
tructure is confirmed by the presence of interference maxima correspon
ding to the number of bilayers in the low angle diffraction data for f
ilms with total film thicknesses less than 33.0 nm.