A. Wolfenden et al., THE RELATION OF DYNAMIC ELASTIC-MODULI, MECHANICAL DAMPING AND MASS DENSITY TO THE MICROSTRUCTURE OF SOME GLASS-MATRIX COMPOSITES, Journal of Materials Science, 29(6), 1994, pp. 1670-1675
Dynamic elastic moduli and mechanical damping were measured with the P
UCOT (piezoelectric ultrasonic composite oscillator) technique at room
temperature for ceramic-matrix composites (CMCs) of the following com
positions: PRD-166 (fibres)/N51A glass (matrix), PRD-166 fibres coated
with SnO2/glass, Nextel 480 fibres/glass, Nextel 480 fibres coated wi
th SnO2/glass, and Nextel 480 fibres coated with BN/glass. The fibres
were continuous, and the volume fractions varied from 0.24 to 0.43. So
me of the mechanical-property measurements correlated with the thickne
ss of one of the coating materials, and with microstructural observati
ons of the misorientation angle of the fibres and normalized fibre len
gth. With increasing volume fractions of fibres, the fraction of broke
n fibres increased. For the PRD-166/glass and PRD-166/SnO2/glass, a su
bstantial fraction of the fibres were misoriented by angles of up to 1
5 degrees. Assessments were made of the measured properties in terms o
f the rule of mixtures and other theoretical estimations.