Yz. Li et al., OBSERVATION OF FRACTURE FEATURES IN FUSED QUARTZ WITH LASER-INDUCED INTERNAL FLAWS, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 176(1-2), 1994, pp. 421-424
Pulsed-laser light was used to generate internal flaws in fused quartz
. The size of the flaw was proportional to the laser pulse energy abov
e a threshold value of 2.5 mJ. Specimens which fractured under four-po
int bending, either from surface origins or from the internal flaws wi
th a size less than 0.25 mm, exhibited the commonly observed fracture
features of sequential mirror, mist, hackle and branching, and the tra
nsition from the mirror to other features was gradual. However, in spe
cimens with internal flaws of a size greater than 0.25 mm, a new ''dem
arcation'' line (a smoothly curved boundary line between the mirror an
d other fracture features) was observed. Its characteristic varied wit
h the flaw size and the relative position along the line. It is sugges
ted that the formation of the demarcation line is caused by the combin
ation of the dynamic process of crack propagation and environmental ef
fects.