A new silicon-silicon bond characterization technique has been demonst
rated. Defect decoration etches can be used to detect weaknesses at th
e bond interface, and the Wright etch was found to be a particularly s
uitable etch. Defects at the bond interface are decorated in the cleav
ed cross section of bonded wafers, and the appearance of the etch figu
res is a qualitative indicator of the bond completeness. The clearest
results are seen when the anneal takes place at or above about 1000-de
grees-C. This technique also decorates the surface of a bonded and thi
nned wafer and can highlight the presence of small voids, undetectable
by IR transmission, that are present at the bond interface. The techn
ique is mainly qualitative in nature but can also give semiquantitativ
e information. In particular, we have estimated an activation energy o
f about 6.1 eV for the mass transport portion during the bonding proce
ss for Si-Si bonds.