J. Schole et C. Schole, GLYCEROL-2-DIETHYL PHOSPHATE BY PHOTOCHEM ICAL-REACTION OF DIHYDROXY ACETONE WITH DIETHYL PHOSPHORIC-ACID, Tetrahedron, 50(12), 1994, pp. 3743-3746
Photochemically excited dihydroxy acetone reacts in 1,2-dimethoxy etha
ne with diethyl phosphoric acid to glycerol-2-diethyl phosphate. The f
ormation of this synthesis product is detected by NMR-spectroscopy, ma
ss spectrometry, phosphate analysis, and chemical synthesis.