Four common techniques for the removal of dissolved oxygen from water
have been examined: boiling at 1 atm, boiling under reduced pressure,
purging with N2 and sonication under reduced pressure. After treatment
, the residual oxygen in solution was analysed by the Winkler method.
Nitrogen purging for 20-40 min at flow rate of 25 mL/s was found to be
the most effective oxygen removal method. Boiling at 1 atm was found
to be the least effective. None of the techniques evaluated here lead
to complete removal of oxygen. The concentration of residual dissolved
oxygen after purging for 20-40 minutes with nitrogen is 0.2-0.4 ppm.