DETERMINATION OF IRON AND LEAD BY FLAME ATOMIC-ABSORPTION SPECTROMETRY AFTER PRECONCENTRATION WITH SEPIOLITE

Authors
TURKER AR BAG H ERDOGAN B
Citation
Ar. Turker et al., DETERMINATION OF IRON AND LEAD BY FLAME ATOMIC-ABSORPTION SPECTROMETRY AFTER PRECONCENTRATION WITH SEPIOLITE, Fresenius' journal of analytical chemistry, 357(3), 1997, pp. 351-353
Citations number
15
Categorie Soggetti
Chemistry Analytical
Journal title
Fresenius' journal of analytical chemistry → ACNP
ISSN journal
09370633
Volume
357
Issue
3
Year of publication
1997
Pages
351 - 353
Database
ISI
SICI code
0937-0633(1997)357:3<351:DOIALB>2.0.ZU;2-S
Abstract
By using a new adsorbent (sepiolite) an adsorption-elution and atomic absorption spectrometric method has been developed for the preconcentr ation and determination of Fe and Pb. Recoveries of the analytes were 82 +/- 3% for Fe and 91 +/- 2% for Pb at 95% confidence level. For Cu it was only 5 +/- 1%. The recovery of iron could be increased to about 97 +/- 1% by complexing with EDTA, the recovery of copper only to 57 +/- 2%. The optimised method was applied to the determination of lead in metal materials (e.g. brass).