THE SYNTHESIS OF NOVEL POLYCYCLIC HETEROCYCLIC RING-SYSTEMS VIA PHOTOCYCLIZATION .14. 14-METHYLBENZO[H]NAPHTHO-[1'2' 4,5]THIENO[2,3-C][1,6]NAPHTHYRIDINE/

Citation
Mj. Musmar et Rn. Castle, THE SYNTHESIS OF NOVEL POLYCYCLIC HETEROCYCLIC RING-SYSTEMS VIA PHOTOCYCLIZATION .14. 14-METHYLBENZO[H]NAPHTHO-[1'2' 4,5]THIENO[2,3-C][1,6]NAPHTHYRIDINE/, Journal of heterocyclic chemistry, 31(2), 1994, pp. 553-555
Citations number
15
Categorie Soggetti
Chemistry Inorganic & Nuclear
ISSN journal
0022152X
Volume
31
Issue
2
Year of publication
1994
Pages
553 - 555
Database
ISI
SICI code
0022-152X(1994)31:2<553:TSONPH>2.0.ZU;2-E
Abstract
]naphtho[1'2':4,5]thieno[2,3-c][1,6]naphthyridine, a novel polycyclic heterocyclic ring system, has been synthesized as the 14-methyl deriva tive 8 in four steps from known intermediates. The structure of 8 is s upported by assignment of the proton and the protonated carbon atoms b y 2D-nmr techniques (COSY and a carbon-hydrogen one-bond coupling expe riment).