Extracts were prepared from the hulls of purple-hulled sunflower, then
processed using clarification, evaporation, and spray drying. Additio
n of citric acid to solvent or raw extract substantially reduced pigme
nt yield, probably by precipitation, but the loss was diminished if ci
tric acid addition was delayed until after evaporation or spray drying
. The highest overall yield, 1.5 to 1.7 mg spray-dried pigment per gra
m of dry hulls, was achieved without addition of citric acid. Pigment
loss was observed at each step, and in the case of evaporation, appear
ed to result mainly from pigment degradation. Although increased brown
ing was observed at each step, reconstituted spray-dried extracts stil
l had an attractive red color.