H. Ohtsuka et al., EFFECT OF GAMMA[--]EPSILON CYCLIC TRANSFORMATIONS ON THE SHAPE-MEMORYCHARACTERISTICS OF AN FE-MN-SI-CR-NI ALLOY, Materials characterization, 32(3), 1994, pp. 229-235
Effects of gamma <-- --> epsilon cyclic transformations on the shape m
emory characteristics have been studied in an Fe-14Mn-6Si-9Cr-5Ni (wt.
%) alloy. First, the effects of two cyclic transformations (one is the
gamma --> epsilon transformation by cooling and its reverse epsilon -
-> gamma transformation by heating, and the other is the gamma --> eps
ilon; stress-induced transformation and its reverse transformation by
heating) on the transformation temperatures were investigated by diffe
rential scanning calorimetry (DSC). M(s) and M(f) temperatures slightl
y decrease with increasing number of the gamma <-- --> epsilon (epsilo
n is formed on cooling) cyclic transformations. The effect of the gamm
a <-- --> epsilon cyclic transformation (epsilon is stress-induced) on
the A(f) temperature is fairly large, and it is remarkably increased
with increasing number of the gamma <-- --> epsilon cyclic transformat
ions. The amount of martensite remarkably increases with increasing nu
mber of the gamma <-- --> epsilon cyclic transformations (epsilon is f
ormed on cooling). Next, the effect of gamma <-- --> epsilon cyclic tr
ansformation (gamma --> epsilon stress-induced transformation and its
reverse transformation by heating under various stresses) on the recov
ery stress was investigated. When the gamma <-- --> epsilon cyclic tra
nsformation is repeated, the recovery stress first increases remarkabl
y and then decreases monotonically irrespective of the stress applied
during the reverse transformation. This increase of recovery stress is
attributed to not only the increase of elongation when the specimen i
s deformed but also to the increase of stacking faults, which act as n
ucleation sites for martensite. The monotonic decrease of recovery str
ess is attributed to the decrease of elongation.