P. Allia et al., SOFT NANOCRYSTALLINE FERROMAGNETIC-ALLOYS WITH IMPROVED DUCTILITY OBTAINED THROUGH DC JOULE HEATING OF AMORPHOUS RIBBONS, Journal of magnetism and magnetic materials, 133(1-3), 1994, pp. 243-247
Nanocrystalline ferromagnetic materials of the type Fe-Nb-Cu-B-Si obta
ined by appropriate furnace annealing of amorphous ribbons display exc
ellent soft magnetic properties but are very brittle. Dc Joule heating
in vacuo allows nanocrystallization to occur in these systems well be
fore the atomic rearrangements in the amorphous phase have been comple
ted, thus partially avoiding the processes leading to sample embrittle
ment. In Fe73.5Cu1Nb3Si13.5B9, the average grain size of Joule-heated
samples is significantly lower than in the furnace-annealed alloy. Nan
ocrystalline strips of this material having very high magnetic permeab
ility and better ductility are therefore obtained. The advantages of t
his rapid heating technique are highlighted.