H. Kanai et al., RECOVERY STUDIES ON DICHLOROMETHANE AQUEOUS PARTITIONING OF PHENOL AND SOME OF ITS ALKYL DERIVATIVES, International journal of environmental analytical chemistry, 53(2), 1993, pp. 151-156
The recoveries of phenol and some of its alkyl derivatives in the prec
oncentration/cleanup of environmental samples using the dichloromethan
e/aqueous partitioning technique is known to be poor. Studying the rec
overy data of phenols which were spiked at different steps of partitio
ning/solvent evaporation procedure, it was found that the poor recover
ies are mainly due to inefficient extraction of phenols into dichlorom
ethane rather than to loss by evaporation or irreversible sorption.