K. Mizuuchi et al., EFFECT OF COLD-WORKING ON THE MECHANICAL- PROPERTIES OF RAPIDLY SOLIDIFIED FE-30CR-5AL ALLOY POWDER CONSOLIDATED BY SHEATH ROLLING, Nippon Kinzoku Gakkaishi, 58(5), 1994, pp. 538-543
Rapidly solidified Fe-30Cr-5Al alloy powders produced by the rotating-
water-atomization-process were sheath-rolled. Three kinds of sheath-ro
lling which are hot sheath-rolling, cold sheath-rolling after hot shea
th-rolling and sintering after cold sheath-rolling were carried out. M
icrostructures and mechanical properties of the sheath-rolled samples
were examined. Sintering after cold sheath-rolling was not effective i
n the breakage of Al2O3 oxide films of the powder particle surface. By
hot sheath-rolling, Al2O3 oxide films were broken or divided to small
pieces and the shape of Al2O3 was changed from plate to granular form
. By hot sheath-rolling, the mean diameter of Al2O3 was 2.5 mum for th
e reduction in cross-sectional area of 80%. Cold sheath-rolling after
hot sheath-rolling were very effective in fine dispersion of Al2O3 oxi
des. By cold sheath-rolling after hot sheath-rolling, the mean diamete
r of Al2O3 was 1.2 mum and the tensile strength was 1060 MPa for the r
eduction in cross-sectional area of 79%. The tensile strength and elon
gation increased drastically with decreasing mean diameter of Al2O3 ox
ides to less than 2 mum.