We have used in situ polar Kerr effect measurements to study the magne
tic anisotropy of MBE-grown X/Co/Y trilayers, where X and Y are combin
ations of the nonmagnetic metals Ag, Au, Cu, or Pd. The competition be
tween the perpendicular anisotropy of the initial underlayer X/Co inte
rface and the in-plane shape anisotropy of the Co film allows us to ad
just the total anisotropy of the uncovered Co to be in plane and of mo
derate strength. In this way, we can measure hard-axis (perpendicular)
polar hysteresis curves in situ as a function of overlayer Y coverage
, and directly deduce the anisotropy field. Polar hysteresis curves we
re measured in situ for systematically varied Co and overlayer Y layer
thicknesses 2 angstrom less-than-or-equal-to t(Co) less-than-or-equal
-to 20 angstrom and 0 angstrom less-than-or-equal-to t(Y) less-than-or
-equal-to 100 angstrom. We find, for particular combinations, the magn
itude of the X/Co/Y perpendicular anisotropy is strongly peaked at app
roximately 1 atomic layer overlayer Y coverage.