Kw. Yang et al., SYNTHESIS, CHARACTERIZATION AND X-RAY CRYSTAL-STRUCTURE OF ZN-II COMPLEX WITH POLY-NITROGEN LIGAND -HB(3,5-ME(2)PZ)(3)]ZN-2-CENTER-DOT-2C(6)H(5)CH(3), Polyhedron, 16(8), 1997, pp. 1297-1300
Di-hydrotris(3,5-dimethylpyrazo-1-yl)borate Zn-II was prepared from KH
B(3,5-Me(2)pz)(3) and Zn(NO3)(2) . 6H(2)O(-) in acetone, characterized
by elemental analysis and H-1 NMK. Crystal structure determination sh
ows that the configuration around the Zn-II center is a slightly disto
rted octahedron. Copyright (C) 1997 Elsevier Science Ltd.