Tj. Bandosz et al., STUDY OF CARBON-SMECTITE COMPOSITES AND CARBONS OBTAINED BY IN-SITU CARBONIZATION OF POLYFURFURYL ALCOHOL, Carbon, 32(4), 1994, pp. 659-664
A sodium form of Wyoming smectite was intercalated with hydroxyaluminu
m cations and saturated with furfuryl alcohol; polymerization and carb
onization were done to obtain carbon-smectite composites. Carbons were
obtained from the smectite inorganic matrices by washing them with HC
l and HF. The synthesized materials were studied by X-ray diffraction,
inverse gas chromatography, DTA, and adsorption of nitrogen and metha
ne. Analyses of data indicate the inorganic matrix acts as a limiting
pore size former in the carbons washed from smectite precursors.