Y. Takasu et al., SUPPORT OF ULTRAFINE PALLADIUM PARTICLES UPON A GLASSY-CARBON SUBSTRATE BY A CHEMICAL METHOD, Bulletin of the Chemical Society of Japan, 67(5), 1994, pp. 1514-1516
Isolated ultrafine palladium particles prepared by a gas-evaporation m
ethod have been chemically supported on a flat glassy carbon substrate
using a silane coupling agent. The modification of the ultrafine pall
adium particles with the silane coupling agent was confirmed by FT-IR
spectroscopy and transmission electron microscopy (TEM). The supported
palladium particles did electrochemical sorption-desorption of hydrog
en in an acidic solution.