Shj. Idziak et al., THE X-RAY SURFACE FORCES APPARATUS - STRUCTURE OF A THIN SMECTIC LIQUID-CRYSTAL FILM UNDER CONFINEMENT, Science, 264(5167), 1994, pp. 1915-1918
An x-ray surface forces apparatus for simultaneously measuring forces
and structures of confined complex fluids under static and flow condit
ions is described. This apparatus, combined with an intense synchrotro
n x-ray source, allows investigation of molecular orientations within
a thin liquid crystal film confined between two shearing mica surfaces
3900 angstroms apart. The layer-forming smectic liquid crystal 8CB (4
-cyano-4'-octylbiphenyl) adopted a series of distinct planar layer ori
entations, including the bulk flow-forbidden b orientation.