K. Higashi et al., DEFORMATION CHARACTERISTICS OF A SUPERPLASTIC ALUMINUM-ALLOY PRODUCEDFROM AMORPHOUS POWDERS, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 182, 1994, pp. 1064-1067
The tensile behaviours of an Al-14wt.%Ni-14wt.%Mm (Mm = misch metal) c
rystalline alloy consolidated from its amorphous powders was character
ized at strain rates between 10(-3) and 100 s-1 at temperatures from 7
73 to 898 K. This alloy exhibited superplasticity at unusually high st
rain rates of nearly 1 s-1 in a temperature range from 848 to 885 K. A
maximum elongation of about 650% was obtained at a constant strain ra
te of 1 s-1 at a very high temperature of 885 K, which was close to or
lower than the melting point. The microstructure of the Al-Ni-Mm crys
talline alloy annealed in the optimum superplastic temperature range c
onsists of grains with a mean size of about 1-2 mum and fine particula
tes a size of about 1.2 mum and a high volume fraction of about 40%. B
y incorporation of the temperature dependence of grain size and shear
modulus into the constitutive equation, the stress exponent and the ac
tivation energy were found to be 2 and 421 kJ mol-1 respectively. It i
s postulated that superplastic flow in the Al-Ni-Mn crystalline alloy
is controlled by a grain boundary sliding mechanism, but the accommoda
tion process remained unclear.