V. Erukhimovitch et J. Baram, ANALYSIS OF SOLIDIFICATION IN THE SPRAY ATOMIZATION PROCESS, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 182, 1994, pp. 1195-1201
Spray atomization is a process for the production of net or near net s
hape products. In this process, a molten stream of metal is disintegra
ted into a fine dispersion of droplets by high velocity gas jets. The
resulting semisolidified droplets are directed towards a substrate whe
re they impact and collect as rapidly solidified splats. High rates of
solidification are achieved as a result of the thinness of the splats
and the rapid heat extraction during fight in the inert atmosphere. I
n this paper, a mathematical formulation for spray atomization, based
on classical nucleation and growth theory and kinetics, is presented.
The model deals with the following: the production of metallic droplet
s by high pressure inert gas atomization, including the droplet-gas in
teraction and the resulting droplet size distribution; the expected mo
de of nucleation of the solid phase, correlated to the droplet size; t
he thermal and solidification histories of the droplets in flight. The
influence of the process parameters, such as the atomization gas pres
sure, the wetting angle, the geometrical features of the atomizer and
feeding crucible, the distance between the atomization nozzles and the
substrate, on the final microstructure is evaluated. As a result of t
his analysis, the optimal choice of the process parameters can be made
, for the production of the desired microstructure.