We have observed x-ray speckle at grazing incidence from gold-coated f
ilms of symmetric diblock copolymers of polystyrene (PS) and polymethy
lmethacrylate (PMMA). The polymer films consisted of micron-sized isla
nds on a uniform surface. Coherent 6-keV photons were selected by mono
chromatizing and collimating the x-ray beam from a bending magnet sync
hrotron source. The visibility of the speckle patterns was enhanced wi
th increasing degrees of spatial coherence of the photons. Speckles du
e to coherent scattering from islands with length scales up to 100 mum
were clearly identified.