PREPARATION AND SPECTROSCOPIC PROPERTIES OF SPIROCYCLIC 1-METHYL-2,4,4,6-TETRAARYL-1,4-DIHYDROPYRIDINES

Authors
BOHM S HOCEK M NEMECEK J HAVLICEK V KUTHAN J
Citation
S. Bohm et al., PREPARATION AND SPECTROSCOPIC PROPERTIES OF SPIROCYCLIC 1-METHYL-2,4,4,6-TETRAARYL-1,4-DIHYDROPYRIDINES, Collection of Czechoslovak Chemical Communications, 59(5), 1994, pp. 1105-1114
Citations number
8
Categorie Soggetti
Chemistry
Journal title
Collection of Czechoslovak Chemical Communications → ACNP
ISSN journal
00100765
Volume
59
Issue
5
Year of publication
1994
Pages
1105 - 1114
Database
ISI
SICI code
0010-0765(1994)59:5<1105:PASPOS>2.0.ZU;2-N
Abstract
1,5-Diones Ib - Ie were converted to spirocyclic 1,4-dihydropyridines IIb - IIe by treatment with methanolic methylamine. The starting diket ones Ib - Ie were obtained from corresponding acetophenones 4-X-C6H4CO Me and fluorenone with sodium amide except of If where only ketone III and 1,4-dione IV were isolated. Molecular spectra (UV-VIS, NMR, IR an d MS) of compounds Ib - Ie, IIa - IIe, III, and IV were assigned and i nterpreted,