In our work a reversible process to creating nanocrystalline Fe73.5Cu1
Nb3Si13.5B9 by annealing the amorphous ribbons was observed. The origi
nal amorphous ribbons of Fe73.5Cu1Nb3Si13.5B9 were annealed at 540-deg
rees-C and at 950-degrees-C respectively as well as melted at 1200-deg
rees-C. Such prepared samples were milled in a vibrational ball mill u
nder the vacuum. The exponential law for decreasing the crystal size w
ith the willing time was observed. The bigger the amount of the amorph
ous rest in material, the shorter is the time of milling for obtaining
the requested crystal size