V. Percec et al., SYNTHESIS AND CHARACTERIZATION OF MONOMETHACRYLATE-FUNCTIONALIZED SELF-ORGANIZING CROWN-ETHER COMPOUNDS, Macromolecular chemistry and physics, 198(2), 1997, pp. 265-277
Synthesis and characterization of methacrylate-monofunctionalized crow
n ether compounds based on derivatives of hydroxymethyl-1,4,7,10,13-pe
ntaoxacyclopentadecane and xymethyl-1,4,7,10,13-pentaoxabenzocyclopent
adecane is described. By differential scanning calorimetry (DSC) and t
hermooptical analysis (TOA) it is shown that the synthesized compounds
and their sodium triflate complexes exhibit columnar mesophases.