Selective area electroless nickel and copper deposition onto the surfa
ce of diamond single crystals and polycrystalline diamond films has be
en realized. Three methods of laser-assisted activation of diamond sur
face were applied: (i) prenucleation of diamond surface with a thin la
yer of palladium catalyst via laser-induced decomposition of a palladi
um acetyl-acetonate [Pd(acac)2] solid film; (ii) deposition of palladi
um by means of the decomposition of Pd(acaC)2 dissolved in dimethylfor
mamide; (iii) laser-induced damage of diamond surface.