APPARATUS FOR THE IN-SITU KINETIC-STUDY OF REACTIONS INVOLVING AIR SENSITIVE MATERIALS USING ENERGY-DISPERSIVE POWER DIFFRACTION

Authors
CLARK SM IRVIN P FLAHERTY J RATHBONE T WONG HV EVANS JSO OHARE D
Citation
Sm. Clark et al., APPARATUS FOR THE IN-SITU KINETIC-STUDY OF REACTIONS INVOLVING AIR SENSITIVE MATERIALS USING ENERGY-DISPERSIVE POWER DIFFRACTION, Review of scientific instruments, 65(7), 1994, pp. 2210-2213
Citations number
10
Categorie Soggetti
Physics, Applied","Instument & Instrumentation
Journal title
Review of scientific instruments → ACNP
ISSN journal
00346748
Volume
65
Issue
7
Year of publication
1994
Pages
2210 - 2213
Database
ISI
SICI code
0034-6748(1994)65:7<2210:AFTIKO>2.0.ZU;2-2
Abstract
A novel sample chamber has been developed for the study of chemical re actions involving air sensitive samples using energy-dispersive powder diffraction. The apparatus consists of a reaction vessel, automatic r eactant dispensing system, heating jacket, stirrer, and gas purge syst em. The use of this apparatus is illustrated with data collected on st ation 9.7 of the UK Synchrotron Radiation Source during a study on the intercalation of cobaltocene into tin disulfide.