C60H2 has been synthesized by ultrasonically irradiating solutions of
C-60 in decahydronaphthalene. This synthesis can be understood as a se
condary reaction arising from the production of atomic hydrogen during
sonolysis of the solvent. Continued sonication results in the eventua
l disappearance of both C-60 and C60H2 from the solution as monitored
by UV-vis spectrophotometry. This disappearance, along with the comple
te absence of more highly hydrogenated derivatives, suggests that the
C-60 experiences a high-energy environment during ultrasonic irradiati
on.