SOLID-PHASE EXTRACTION AND LIQUID-CHROMATOGRAPHY ANALYSIS OF NITROFURAN COMPOUNDS IN MEAT

Authors
POSYNIAK A SEMENIUK S NIEDZIELSKA J ZMUDZKI J
Citation
A. Posyniak et al., SOLID-PHASE EXTRACTION AND LIQUID-CHROMATOGRAPHY ANALYSIS OF NITROFURAN COMPOUNDS IN MEAT, Chemia Analityczna, 39(3), 1994, pp. 289-294
Citations number
7
Categorie Soggetti
Chemistry Analytical
Journal title
Chemia Analityczna → ACNP
ISSN journal
00092223
Volume
39
Issue
3
Year of publication
1994
Pages
289 - 294
Database
ISI
SICI code
0009-2223(1994)39:3<289:SEALAO>2.0.ZU;2-O
Abstract
Nitrofurans were extracted from animal tissues with acetonitrile and c lean-up by solid phase extraction (SPE) procedure. For dean-up C18 col umns were used and retained drugs were eluted with acetonitrile contai ning 0.1 %(V/V) ammonia. The liquid chromatography (LC) separation was carried out on a C18 analytical column using acetate buffer and aceto nitrile as the mobile phase and a UV-VIS detector. Recoveries from spi ked muscles were above 80 %, and detection limit was 2 ng g-1 of tissu e.