Ea. Osipova et al., DETERMINATION OF GERMANIUM IN SEMICONDUCTOR-MATERIALS BY THE ADSORPTION INVERSION VOLTAMPEROMETRIC METHOD, Industrial laboratory, 60(2), 1994, pp. 82-83
The possibility of voltamperometric determination of germanium in semi
conductor Pb1-xGexTe materials using the reaction of formation of moly
bdogermanic heteropolyacids (MGA) and adsorption concentration of the
latter on the surface of a carbon paste electrode is studied. The meth
od developed offers the advantage of revealing fine differences in the
composition of analyzed specimens, which is impossible to do by X-ray
phase analysis. The method is simple in application and makes it poss
ible to analyze milligram-weight samples.