The role of microstructural scale on deformation-microfracture damage
induced by contact with spheres is investigated in monophase alumina c
eramics over a range 3-48 mum in grain size. Measurement of a universa
l indentation stress-strain curve indicates a critical contact pressur
e almost-equal-to 5 GPa, above which irreversible deformation occurs i
n alumina. A novel sectioning technique identifies the deformation ele
ments as intragrain shear faults, predominantly crystallographic twins
, within a confining subsurface zone of intense compression-shear stre
ss. The twins concentrate the shear stresses at the grain boundaries a
nd, above a threshold grain size, initiate tensile intergranular micro
cracks. Below this threshold size, classical Hertzian cone fractures i
nitiate outside the contact circle. Above the threshold, the density a
nd scale of subsurface-zone microcracks increase dramatically with inc
reasing grain size, ultimately dominating the cone fractures. The dama
ge process is stochastic, highlighting the microstructural discretenes
s of the initial deformation field; those grains which lie in the uppe
r tail of the grain-size distribution and which have favorable crystal
lographic orientation relative to local shear stresses in the contact
field are preferentially activated. Initial flaw state is not an impor
tant factor, because the contact process creates its own flaw populati
on. These and other generic features of the damage process will be dis
cussed in relation to microstructural design of polycrystalline cerami
cs.