Thick thermal barrier coatings (TTBCs) of Plasma-sprayed 8% Y2O3-ZrO2
were fatigued in compression as part of a reliability and durability s
tudy to evaluate their potential use in high-performance diesel engine
s. Test specimens were designed to test the bulk ceramic uniaxially, i
ndependent of the substrate. A test machine was designed to alleviate
the mechanical gripping and alignment difficulties associated with cyc
lically stressing brittle ceramics in compression. Higher fatigue limi
ts, 375 vs 200 MPa, were observed at 800-degrees-C than at room temper
ature. Specimens tested at room temperature after high-temperature com
pressive cycling also had higher fatigue limits, indicating that the s
trengthening was permanent. At temperatures of 800-degrees-C, the coat
ings showed evidence of low-temperature, pressure-induced sintering. T
he extent to which sintering occurred was determined by studying the c
hange in the elastic modulus as a result of the application of varying
temperatures and static stresses.