In order to determine the mercury content present as a contaminant in
samples of bleach used in water and food disinfection, a method for sa
mple treatment using chloridric acid to eliminate the chlorine was pro
posed. The technique of cold vapour atomic absorption spectrophotometr
y, used to quantify the mercury, showed a recovery of 103%. Sixty nine
samples of bleach were analysed and the values found for the median a
nd 90th percentil were respectively, 15 and 67 mug/L. According to the
values of residual mercury found and using the quantities of bleach r
ecommended by the Brazilian Sanitary Authorities, the use of these dis
infectants offers no risk to human health.