SILICON-COMPOUNDS WITH STRONG INTRAMOLECULAR STERIC INTERACTIONS .53.CRYSTAL-STRUCTURE OF XYL-4,5-DIPHENYL-1-OXA-2-SILA-3-AZA-4-CYCLOPENTENE

Authors
PETERS K PETERS EM VONSCHNERING HG PIEL H WEIDENBRUCH M
Citation
K. Peters et al., SILICON-COMPOUNDS WITH STRONG INTRAMOLECULAR STERIC INTERACTIONS .53.CRYSTAL-STRUCTURE OF XYL-4,5-DIPHENYL-1-OXA-2-SILA-3-AZA-4-CYCLOPENTENE, Zeitschrift fur Kristallographie, 209(7), 1994, pp. 611-612
Citations number
5
Categorie Soggetti
Crystallography
Journal title
Zeitschrift fur Kristallographie → ACNP
ISSN journal
00442968
Volume
209
Issue
7
Year of publication
1994
Pages
611 - 612
Database
ISI
SICI code
0044-2968(1994)209:7<611:SWSISI>2.0.ZU;2-3
Abstract
The title compound was synthesized by photolysis of hexa-tert-butylcyc lotrisilane in the presence of N-cyclohexyl-2,3-diphenyl-alpha-ketoimi ne. It crystallizes from n-pentane monoclinically in the space group P 2(1)/a with a = 1823.2(1) pm, b = 1041.1(1) pm, c = 1366.3(1) pm and b eta = 96.52(1)-degrees