T. Hashishin et al., PREPARATION OF TITANIUM-DIOXIDE FIBERS USING SODIUM ALGINATE, Nippon Seramikkusu Kyokai gakujutsu ronbunshi, 105(3), 1997, pp. 206-209
A new method for preparing titanium dioxide fibers using sodium algina
te has been developed. Titanium dioxide fibers were obtained by heatin
g alginic acid fibers containing titanium dioxide particles (precursor
s) in air, which were produced from titanium dioxide sol and sodium al
ginate as starting materials. X-ray microanalysis (EPMA) of the cross
section of the precursors showed that titanium dioxide particles were
homogeneously distributed from the surface to the center of the precur
sors. When the precursors were heated (holding time: Ih, temperature:
900 degrees C), phase transition from anatase to rutile was observed.
In addition, the pores between particles became very small as heating
temperature was increased above at 900 degrees C, which indicates that
the particles become densely distributed.