Ms. Louisweber et al., TRANSPORT-PROPERTIES OF AN ENGINEERED [001]-TILT SERIES IN BULK YBA2CU3O7-X BICRYSTALS, Physical review. B, Condensed matter, 54(22), 1996, pp. 16238-16245
Single grain boundaries (GB's) of an engineered [001] tilt series of b
ulk YBa2Cu3O7-x (YBCO) bicrystals were electrically characterized to p
robe the intrinsic and extrinsic factors influencing GB properties of
bulk melt-processed (MP) YBCO. The bicrystal series ranged from 1.5 de
grees to 45 degrees misorientation angle and displayed tendencies simi
lar to those of thin film GB's at 77 K in self-field. Subtle differenc
es between thin film and bulk GB transport behavior that were observed
may be attributed to the thin film substrate. The dependence of norma
l-state resistance (R(n)) at 77 K on the [001] tilt angle has been not
ed. An anticorrelation between R(n) and critical current (I-c) exists
such that the product, I(c)R(n), of each bicrystal from 10 degrees to
45 degrees falls within a narrow band of 10 to 20 mu V. Such a narrow
characteristic voltage range suggests highly reproducible growth condi
tions. It is also reasonable to suggest that naturally grown boundarie
s in bulk MP YBCO have more uniform GB character than their thin film
counterparts. This advantageous growth technique allows us to further
probe the role of the GB plane in influencing transport properties.