Tialite, beta-Al2TiO5, a low expansion material, has been synthesised
by the combustion of corresponding metal nitrates and carbohydrazide (
CH) or urea redox mixtures at 500-degrees-C. As prepared powders conta
ined tialite, rutile, and corundum in the mole ratios of 50:25:25 (CH)
and 20:40:40 (urea). The combustion derived powders, when calcined 30
min at 1300-degrees-C, gave single phase beta-tialite having a surfac
e area of 20-25 m2 g-1 and a particle size of 0.79-1.03 mum.