Cm. Romokroger, ION-INDUCED X-RAY-EMISSION AND ELECTRON-MICROSCOPY FOR THE INVESTIGATION OF MICROPARTICLES, Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 85(1-4), 1994, pp. 845-848
Micro-particles deposited over membrane Nuclepore filters or other smo
oth surfaces are well suited to be analyzed by PIXE (particle induced
X-ray emission) and by electron probe techniques. The effect of the si
ze of micro-particles on a surface sample when analyzed by macro-PIXE
[11] is discussed. To analyze individual particles (sizes, distributio
n, geometry, etc.) electron microscopy is the most accepted technique.
A way to complement macro-PIXE and microscopy is described which pres
ents some advantages over the sophisticated micro-PIXE systems. Second
ary electron microscopy (SEM), electron micro-probe and optical micros
copy were applied to aerosol and other similar samples. SEM micrograph
s served to define some physical properties of particles through a dev
eloping image processing program.