SIMULTANEOUS DETERMINATION OF ORGANIC IONIC LEAD AND MERCURY SPECIES USING HPLC

Authors
CAMMANN K ROBECKE M BETTMER J
Citation
K. Cammann et al., SIMULTANEOUS DETERMINATION OF ORGANIC IONIC LEAD AND MERCURY SPECIES USING HPLC, Fresenius' journal of analytical chemistry, 350(1-2), 1994, pp. 30-33
Citations number
10
Categorie Soggetti
Chemistry Analytical
Journal title
Fresenius' journal of analytical chemistry → ACNP
ISSN journal
09370633
Volume
350
Issue
1-2
Year of publication
1994
Pages
30 - 33
Database
ISI
SICI code
0937-0633(1994)350:1-2<30:SDOOIL>2.0.ZU;2-1
Abstract
A reversed-phase HPLC separation of organic ionic lead and mercury spe cies has been achieved by using pre and on-column derivatisation with methyl thioglycolate. The separation parameters have been optimized an d shown to permit a reproducible determination. For the enrichment of the compounds from water samples, the complexed organometallic species are concentrated on a precolumn. A recovery of 70 to 80% is achieved by using this one-line enrichment method.