P. Masse et al., INTERFACE CHARACTERIZATION BY PULL-OUT TEST BETWEEN HIGH-MODULUS POLYETHYLENE FIBER AND AN UNSATURATED POLYESTER RESIN, Journal de physique. IV, 3(C7), 1993, pp. 1661-1664
The observation of the pull-out conditions for a monofilament outside
a matrix has been applied to a wide variety of organic or inorganic ma
terials, as a direct method of interface characterization. In the case
of High Modulus PolyEthylene (HMPE) it has been demonstrated that oxy
gen plasma treatments or gamma irradiation modify the fibre surface pr
operties and improve the adhesion between the fibre and a resin. In th
is study, the effect of different plasma treatment times and the irrad
iation conditions leading to different gel fractions have been tested.
For plasma treatments, an appreciable improvement occurs even for the
lower residence times (2 sec). The gamma irradiation has only the sam
e efficiency for the condition leading to a high gel fraction (0.75).
These results agree with InterLaminar Shear Strengths (ILSS) values me
asured in three-point bending on HMPE/epoxy laminates.