L. Gunaratnam et K. Himberg, THE IDENTIFICATION OF GUNSHOT RESIDUE PARTICLES FROM LEAD-FREE SINTOXAMMUNITION, Journal of forensic sciences, 39(2), 1994, pp. 532-536
Scanning electron microscopy combined with energy dispersive X-ray ana
lysis (SEM/EDX) was used to identify the gunshot residue (GSR) particl
es discharged by lead-free Sintox ammunition. Sintox GSR particles are
characterized by spheroidal particles mainly consisting of titanium (
Ti) and zinc (Zn). The results obtained in this study are in agreement
with the hypothesis that GSR particles are formed by rapid condensati
on and solidification of vaporized and molten primer and bullet materi
als as a result of sudden temperature quench. The surface morphology o
f Ti-Zn particles is an essential criterion for their identification a
s gunshot residue particles and for discrimination against Ti-Zn envir
onmental particles.