CRYSTAL-STRUCTURE AND MOLECULAR-STRUCTURE OF TRANS-DICHLORO-METHYL, TRANS-DIMETHYL, TRANS-BIS(QUINOLINE N-OXIDE)TIN

Authors
NG SW DAS VGK
Citation
Sw. Ng et Vgk. Das, CRYSTAL-STRUCTURE AND MOLECULAR-STRUCTURE OF TRANS-DICHLORO-METHYL, TRANS-DIMETHYL, TRANS-BIS(QUINOLINE N-OXIDE)TIN, Zeitschrift fur Kristallographie, 209(9), 1994, pp. 744-745
Citations number
15
Categorie Soggetti
Crystallography
Journal title
Zeitschrift fur Kristallographie → ACNP
ISSN journal
00442968
Volume
209
Issue
9
Year of publication
1994
Pages
744 - 745
Database
ISI
SICI code
0044-2968(1994)209:9<744:CAMOTT>2.0.ZU;2-O
Abstract
Dimethyltin dichloride forms with quinoline N-oxide a stereochemically crowded all-trans-octahedral 1/2 molecular complex that crystallizes in the monoclinic P2(1)/n space group (a = 10.022(1) angstrom, b = 10. 4374(8) angstrom, c = 10.871(2) angstrom; beta = 116.674(6)-degrees). Anisotropic refinement of non-hydrogen and isotropic refinement of hyd rogen atoms converged to R = 0.018 for 1537 independent I greater-than -or-equal-to 3sigma(I) reflections.