CRYSTAL-STRUCTURE AND RAMAN-SPECTRUM OF N ITRONIUMTRINITROSYLPENTANITRATOZIRCONATE, NO2(NO)(3)[ZR(NO3)(5)](4)

Authors
KAISER V EBINAL S MENZEL F STUMPP E
Citation
V. Kaiser et al., CRYSTAL-STRUCTURE AND RAMAN-SPECTRUM OF N ITRONIUMTRINITROSYLPENTANITRATOZIRCONATE, NO2(NO)(3)[ZR(NO3)(5)](4), Zeitschrift fur anorganische und allgemeine Chemie, 623(3), 1997, pp. 449-455
Citations number
21
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Zeitschrift fur anorganische und allgemeine Chemie
ISSN journal
00442313 → ACNP
Volume
623
Issue
3
Year of publication
1997
Pages
449 - 455
Database
ISI
SICI code
0044-2313(1997)623:3<449:CARONI>2.0.ZU;2-J
Abstract
Single crystals of the triclinic compound NO2(NO)(3)[Zr(NO3)(5)](4) (a = 1376.3(6), b = 1376.9(11), c = 1632.0(7) pm, alpha = 114.63 degrees (5), beta = 114.90 degrees(4), gamma = 90.34 degrees(5); P1, Z = 2) ha ve been investigated by x-ray diffraction and Raman spectroscopy. The crystals were prepared by reaction of N2O5 with ZrCl4. The product was sublimed and crystallised in nitroethane.