Wj. Kim et al., INGOT PROCESSING AS AN ALTERNATIVE TO POWDER PROCESSING FOR ACHIEVINGSUPERPLASTICITY IN CERAMICS, Nippon Seramikkusu Kyokai gakujutsu ronbunshi, 102(9), 1994, pp. 835-843
The mechanical behavior of an iron carbide base material processed by
an ingot route was compared with that of the same composition material
processed by a powder route. Thermo-mechanical processing routes have
been developed to refine the coarse as-cast ingot microstructure. Str
uctural refinement is a result of creation of strain-free regions by c
arbon dissolution from high strain energy subgrain boundaries and slip
bands. The ingot-processed iron carbide material exhibits superplasti
c behavior and deforms by the same grain boundary sliding mechanism as
for the powder-processed material. It is proposed that thermo-mechani
cal processing of ingot-cast eutectic-composition ceramics to achieve
a superplastic structure is feasible.